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05-12-2006, 09:31 PM #33
Senior Member
Cookin some LSD
[QUOTE=God v2.0]You guys are fucking pussies, with like 2 grand i could make a huge batch of LSD and it would sell for massive amounts of money prolly somewhere around 10-12k. here i can translate most of the first paragraph:
SYNTHESIS : A solution of 6.7 g KOH in 100 mL H2O, (mix 6.5grams of Potassium Hydroxide in 100 mL of water) under an inert atmosphere and magnetically stirred, was brought to 75 °C, and 10 g ergotamine tartrate (ET) added Ergotamine is a mold found on rye and other grains, its an alkalai thats poisonous and pretty much makes ya go crazy, called st elmo's fire i believe, this substance is controlled. The reaction mixture turned yellow as the ergotamine went into solution over the course of 1 h. The stirring was continued for an additional 3 h. The reaction mixture was cooled to about 10 °C with an external ice bath, and acidified to a pH of about 3.0 by the dropwise addition of 2.5 N H2SO4 you add 1 drop at a time of sulfuric acid (be careful with this shit it will eat right through you LITTERALLY) until the pH is 3.0, just use little pH tester strips for a cheap, fairly accurate reading . White solids started to appear early in the neutralization; approximately 60 mL of sulfuric acid was required. The reaction mixture was cooled overnight, the solids removed by filtration, and the filter cake washed with 10 mL Et2O i think its ethanol. The dry solids were transferred to a beaker, suspended in 50 mL 15 % ammonia in anhydrous ethanol, stirred for 1 h, and separated by decantation http://en.wikipedia.org/wiki/Decantation. This extraction was repeated, and the original decantation and the second extract combined and filtered to remove a few hundred milligrams of unwanted solids. The clear filtrate was stripped of solvent under vacuum, a really good food dehydrator can accomplish this step the residual solids dissolved in 50 mL of 1% aqueous ammonia this is .5 mL of ammonia and 49.5 of water, and this solution was acidified as before with 2.5 N H2SO4 more sulfuric acid baby!. The precipitated solids were removed by filtration and washed with Et2O i cant find out what Et2O is but i think its ethanol can anyone confirm? until free of color. After drying under vacuum to a constant weight, there was obtained 3.5 g of d-lysergic acid hydrate, which should be stored in a dark, sealed container.
its easy
srry about double post[/QUOTE Yes, ethanol. But ergatomine is not mold, but rather one a shitload of chems in that mold. A really solvent intense extraction would be required. Anyone trying to order ergo-anything should have an attorney on speed dial. Getting enough ergot fungus to do anything would involve growing a crop of rye, getting a sample of the fungus, infect the rye, harvest a couple acres of grain by hand, then you move to the extraction, preferably somewhere that the smell of a boatload of ether won't attract attention. Do all that right, you have ONE of the almost impossible to get chems, then you get to make diethylamine. Meanwhile, back in the real world...\"Rightful liberty is unobstructed action according to our will, within limits drawn by the equal rights of others. I do not add \"within the limits of the law\', because law if often but the tyrant\'s will, and always so when it violates the rights of the individual.\"-Thomas Jefferson.
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