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  1.     
    #1
    Junior Member

    Acetylated THC

    I read somewhere about a guy in Florida who's house got raided and they found him making acetylated cannobanoids. Apperently he reacted purified hash oil with glacial acetic acid. They said the modified cannobanoids were twice as potent as normal cannobanoid oil. Has anyone heard of chemically modifying cannobanoids before? I also read something about a phospate salt of THC that is water soluble, making it possible to snort it or absorb it under the tongue, and theoretically, cannobanoid salts will not test positive for marijuana.

    Some of you may not consider this appropriate since it is technically talking about something that isn't marijuana, but I believe it is appropriate since it presents another way to make taking cannobanoids more efficient and convenient.

    Certainly some of you would be interested in making your stash last twice as long, and be undetectable and in snortable or smokable form. Of course, if anyone were to find a tec. on how to make it, it should only be attempted by a skilled chemist. Glacial acetic acid isn't anything to fuck with.
    caspr420 Reviewed by caspr420 on . Acetylated THC I read somewhere about a guy in Florida who's house got raided and they found him making acetylated cannobanoids. Apperently he reacted purified hash oil with glacial acetic acid. They said the modified cannobanoids were twice as potent as normal cannobanoid oil. Has anyone heard of chemically modifying cannobanoids before? I also read something about a phospate salt of THC that is water soluble, making it possible to snort it or absorb it under the tongue, and theoretically, cannobanoid salts Rating: 5

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  3.     
    #2
    Senior Member

    Acetylated THC

    Well... i did read something about this some time ago at:

    Robert A. Nelson: Hemp Husbandry ~ Cannabinoid Chemistry (Ch 6)

    This link has some old informations, so surely there are another methods for making this THC-acetate.

    Quote Originally Posted by The link above
    THC gives an acetate (ATHC) which is as potent as THC. The mental effects are quite subtle and pleasant. Wohlner, et al., prepared ATHC by refluxing the crude distillate of cannabis oil with approximately 3 volumes of acetic anhydride. It is purified by distillation i.v. or with steam.

    Cahn prepared ATHC thus: add 150 ml acetyl chloride (dropwise with stirring and cooling) to 185 gr crude resin in 500 ml dry pyridine. Crystals may separate during the addition, or on standing a few hours at room temperature. Pour the mixture into dilute hydrochloric acid/ice. Separate the oil, then dissolve it in ether. Wash this solution with dilute acid, then with aqueous sodium carbonate, and again with water. Dry the solution with calcium chloride. Strip the solvent and distill the residue (240-270 C°/20 mm). The mixture of acetylated cannabinoids is separated by dissolving 2 gr in 100 ml benzene and chromatography over silica (150-200 mesh). Elute with 800 ml benzene. Combine the washings and the original effluent solutions, then strip the benzene i.v. to recover about 60% yield of light yellow oil. The material remaining on the column contains CBD and other cannabinoid acetates which can be recovered with ethanol and worked up.(21)

  4.     
    #3
    Senior Member

    Acetylated THC

    Quote Originally Posted by Coelho
    Wohlner, et al., prepared ATHC by refluxing the crude distillate of cannabis oil with approximately 3 volumes of acetic anhydride. It is purified by distillation i.v. or with steam.

    Cahn prepared ATHC thus: add 150 ml acetyl chloride (dropwise with stirring and cooling) to 185 gr crude resin in 500 ml dry pyridine. Crystals may separate during the addition, or on standing a few hours at room temperature. Pour the mixture into dilute hydrochloric acid/ice. Separate the oil, then dissolve it in ether. Wash this solution with dilute acid, then with aqueous sodium carbonate, and again with water. Dry the solution with calcium chloride. Strip the solvent and distill the residue (240-270 C°/20 mm). The mixture of acetylated cannabinoids is separated by dissolving 2 gr in 100 ml benzene and chromatography over silica (150-200 mesh). Elute with 800 ml benzene. Combine the washings and the original effluent solutions, then strip the benzene i.v. to recover about 60% yield of light yellow oil. The material remaining on the column contains CBD and other cannabinoid acetates which can be recovered with ethanol and worked up.(21)

    Does the above sound so extremely complicated, difficult and ridiculously expensive to anyone else?

    Holy Hell Coelho, May the Force Be With You!

  5.     
    #4
    Senior Member

    Acetylated THC

    Good luck getting acetic anhyride, its used to process heroin so unless you do that also, you're shit out of luck.

  6.     
    #5
    Junior Member

    Acetylated THC

    Some steps could be omitted or changed. I bet you wouldn't even need benzene. And acetic anhydride can be made from acetates (that you make from glacial acetic acid) with a simple distillation rig and some other glassware. I'm just saying, if you have the stuff and the ambition, it might be something of interest.
    Maybe my scientist buddy SWIM will try it and tell you guys how it is.

    Thanks to roguesci.org he knows alot about home chemistry .

  7.     
    #6
    Member

    Acetylated THC

    I don't want to "make some".. I want to "get some"!
    I am in AZ.. an MMJ state.. and dispensaries are not open yet.
    I want to "drip" my cannabis (acetalized) in an ecig!

  8.     
    #7
    Senior Member

    Acetylated THC

    I'm sure it would be very expensive to make, an oz of bud only makes a small amount of hash oil.

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